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Dell JSM-6060LV - page 1
JEOL JSM-6060L V SCANNING ELECTR ON MICR OSCOPE Insert Nickname Her e Operating Instr uctions ...
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Dell JSM-6060LV - page 2
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 1 T able of Contents 1 INTRODUCTION Safety 3 2 BACKGROUND Background Inf ormation 4 References 4 3 SAMPLES Sample Holders 7 Sample Preparation 7 4 OPERATION Instrume nt Startup 8 Sample Loading 8 Getting an Image 9 Moving Around 9 Image Scanning 10 Zooming In (or Out) 10 Other Toolbar But tons 10 System ...
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Dell JSM-6060LV - page 3
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 2 Introduction he JEOL JSM-6060LV is a sta te-of-the-art scanning electron microscope that features a low vacuum for observation of non-conductive specimens, a fully automated electron gun, a backscattered electron detector for at omic number contra st imaging, fully integrated digital control, motorized ...
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Dell JSM-6060LV - page 4
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 3 Background The scanning electron microscope (SEM) is one of the most versatile instruments for the examination and analysis of the microstructural ch aracteristics of solids. Although the SEM and optical microscope share the same primary functi on – making microstructura l features and objects visibl ...
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Dell JSM-6060LV - page 5
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 4 Figure 2. Schematic illustration of SEM electron The basic components of a SEM are the vacuum system, electron gun, lens system, electron detector, imaging system, and the electronics asso ciate d with these components. The vacuum system is necessary to minimize the interferen ce of air particles with ...
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Dell JSM-6060LV - page 6
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 5 Samples he JEOL JSM-6060LV in stan dard high vacuum operatin g mode can handle a variety of sample types. The low vacuum mode enables the instrument to handle non- conductive samples, including organic materia ls (polymers, etc.), ceramics and glasses, and biological samples. Sample Holder s Please use ...
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Dell JSM-6060LV - page 7
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 6 2. Remove excess lint, dust, moisture, and other debr is from your specimen, unless you want to examine those things. 3. Use the sputter coater to create a conductive gold coating on the surface of your sample. See separate operating instructions for the sputter coater. 4. After coating your sample, us ...
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Dell JSM-6060LV - page 8
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 7 Instrument Operation his section will walk you through the basic operation of the scanning electron microscope. You will follow a se ries of t asks that includes • Powering up the instrument, • Loadin g your sample, • Evacuating the chamber, • Turning on the electron gun, and • Gazing at some ...
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Dell JSM-6060LV - page 9
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 8 6. Close the chamber door by gently pushing it fo rward until it stops. 7. Press and hold the EVAC button (on the front of the instrument) until it lights up green. 8. WAIT for evacuation of the chamber (about 1 minut e). While you’re wait ing, go to the next section – Software. Getting an Image 1. ...
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Dell JSM-6060LV - page 10
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 9 3. Tilt. Turn the knob at the lower right side of the chamber d oor assembly to tilt your specimen. BE CAREF UL when adjusting the sample tilt – you don’t want to run your sample into anything inside the column. 4. Height . Sample height may be changed by manual ly adjusting the y-axis position kno ...
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Dell JSM-6060LV - page 11
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 10 Photography cquiring an image from the SEM is relative ly easy, but there are quite a few options for live image scanning and corresponding image resolution. This section outlines several options for acquiring digita l images of different resolutions, and it provides a few general tips fo r good SEM p ...
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Dell JSM-6060LV - page 12
JEOL JSM-6060LV SCANNING ELECTRON MICROSCOPE 11 4. Once the image is frozen, click the Save button above the image, select a save directory, type a filename, select a fi le format, and click Save . Higher R esolution (slow er) Photos 1. Press the green Scan2 button on the toolbar. 2. Carefully adjust the focus and stigmation settings at a higher ma ...
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